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I am a biker and I always want to date a biker too. To test the suitability of our system and the U-Pb age reproducibility of the Concordia ages, zircon samples covering a wide age range from 2. The analyzed samples comprised the following: Zircons were separated by conventional procedures using heavy liquids and magnetic separator after the concentration by hand panning. Handpicked zircons were mounted in epoxy discs along with zircon standards, ground and polished, microphotographed in transmitted and reflected light, and and their internal zoning imaged by cathodoluminescence CL using scanning electron microscope.

Analytical methods and data treatment can be found elsewhere Compston et al. The reduction of raw data and age calculation were carried out using Squid 2. We have tried to do the spot with the same size or somewhat larger and at the same site or close as regarding those did with SHRIMP. In some cases, due to the low content of Pb, either larger spots were used or increased the number of spots in the same zircon phase in order to get more precise data with the LAM method see discussion of results.

Laser-induced elemental fractional and instrumental mass discrimination were corrected using the reference zircon GJ-1 Jackson et al.

Two GJ-1 analyses were measured after every four or ten sample zircon spots. The external error was calculated after the propagation error of the GJ-1 mean and the individual sample zircon or spot. The collector configuration used for simultaneous measurements of Th, U, Pb and Hg isotopes is as follows: The gain calibration of Faraday cups and the cross calibration between the L4 cup against the MIC3, 4 and 6 were carried out before the laser running was started.

Because the multicollector system involves 3 ion counters and 5 conventional Faraday collectors, the gain and cross calibration must be performed routinely. The gain factor used to calibrate the Faraday measurements is calculated by applying a constant signal of The cross calibration used to calculate the necessary conversion factors voltage to cps is achieved using a ppt Neptune solution with the addition of ppt Th and an efficient nebulizer system.

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The various ratios are obtained simultaneously and appropriately corrected. However, because of inherent elemental and isotopic fractionations during laser ablation, these ratios vary during the analysis and require different approaches to estimate reliable data. Pb is more volatile than U, which condenses progressively on the walls of the pit formed during the laser ablation process.

Outliers that do not show a good alignment are also discarded. These ratios are usually quite close to the expected values. The conversion factors are calculated based on the available data for the standard used and applied to unknown samples. Thus, a homogeneous standard is of paramount importance. Mass bias correction, external correction, and laser conditions. The isotope ratios and inter-element fractionation of data obtained by the MC-ICP-MS instrument were evaluated by interspersing the GJ-1 standard zircon on every set of 4, 6, 8 or 10 zircon samples spots.

The number of analyzed spots varied depending on the zircon homogeneity and the amount of Pb and U in the zircon. The GJ-1 standard zircon was used to estimate the necessary corrections for the external corrections and the internal instrumental fractionation. The GJ-1 zircon and sample were assembled in the same mounting. The repetition rate of the laser was 10 Hz. The energy varied from 0. The data acquisition occurred in 50 cycles of 1. For every standard and sample set, blank values in the same conditions as the standard and sample were also measured.

The average blank values were subtracted from all individual cycle measurements. Laser operation conditions are shown in Table I.

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The usual method for common-lead corrections on zircon grains based on the non-radiogenic Pb isotope is not appropriate when using the laser technique because the Pb signal is strongly affected by Hg. After the Hg correction based on Hg is measured, the common Pb is insignificant in most situations. For instance, a typical signal intensity of the Hg during laser ablation of the standard zircon is in the cps range, and the calculated count rate for Pb is less than the statistical error of ca.

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